2-甲氧基-6-甲基苯甲醛合成路线 （共 15 条）
反应条件
T=200°C; 26 h; sealed tube;
参考文献
Kametani, Tetsuji; Honda, Toshio; Matsumoto, Hiroo; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1383 - 1385
反应条件
boron tribromide in dichloromethane
T=0°C; 1.5 h;
参考文献
Pu; Scripko; Huang
Journal of Labelled Compounds and Radiopharmaceuticals, 1995 , vol. 36, # 12 p. 1183 - 1191
反应条件
1: 94 percent / diethyl ether
2: 81 percent / CrO3, H2SO4 / acetone
View Scheme
参考文献
Michael, Joseph P.; Parsons, Andrew S.
Tetrahedron, 1996 , vol. 52, # 6 p. 2199 - 2216
反应条件
manganese(IV) oxide; magnesium
1.) ether, 30 min; reflux, 30 min, 2.) benzene, reflux, 10 h; Yield given. Multistep reaction;
参考文献
Carter, Stephen D.; Wallace, Timothy W.
Synthesis, 1983 , # 12 p. 1000 - 1002
反应条件
1: 1.) Mg, 2.) MnO2 / 1.) ether, 30 min; reflux, 30 min, 2.) benzene, reflux, 10 h
2: boron tribromide / CH2Cl2 / 20 h / Ambient temperature
View Scheme
参考文献
Carter, Stephen D.; Wallace, Timothy W.
Synthesis, 1983 , # 12 p. 1000 - 1002
