苄氧羰基-甘氨酰-D-苯丙氨酸合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in methanol; water; acetic acid Yield given;
参考文献
Owa, Takashi; Otsuka, Masami; Ohno, Masaji
Chemistry Letters, 1988 , p. 83 - 86
反应条件
1: 89 percent / DCC / CHCl3; tetrahydrofuran / -10 °C
2: 1 M NaOH / methanol
View Scheme
参考文献
Owa, Takashi; Otsuka, Masami; Ohno, Masaji
Chemistry Letters, 1988 , p. 83 - 86
反应条件
sodium hydroxide in methanol
参考文献
Owa, Takashi; Otsuka, Masami; Ohno, Masaji
Chemistry Letters, 1988 , p. 83 - 86
反应条件
1: 89 percent / DCC / CHCl3; tetrahydrofuran / -10 °C
2: 1 M NaOH / methanol
View Scheme
参考文献
Owa, Takashi; Otsuka, Masami; Ohno, Masaji
Chemistry Letters, 1988 , p. 83 - 86
反应条件
1: 95 percent / Jones' reagent / acetone / 3 h / 0 °C
2: 63 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
3: Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: 38 percent / NaHCO3 / CH2Cl2; H2O / Ambient temperature
2: 95 percent / Jones' reagent / acetone / 3 h / 0 °C
3: 63 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
4: Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
diethyl ether; potassium hydrogencarbonate
Behandeln des Reaktionsprodukts mit wss.-aethanol. Natronlauge;
参考文献
Neurath; Elkins; Kaufman
Journal of Biological Chemistry, 1947 , vol. 170, p. 221,222
反应条件
jones' reagent
Yield given. Yields of byproduct given;
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
