1: n-BuLi / light petroleum; hexane / 0 deg C, 15 min, RT., 30 min
2: 84 percent / n-BuLi / hexane; light petroleum / - 78 deg C to -10 deg C, within 1.5 h
3: H2 / Lindlar cat. / diethyl ether; hexane / 0.25 h / Ambient temperature
View Scheme
参考文献
Pelter, Andrew; Al-Bayati, Redha I. H.; Ayoub, Miqdad T.; Lewis, Wynn; Pardasani, Pushpa; Hansel, Rudolf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 717 - 742
1: 84 percent / n-BuLi / hexane; light petroleum / - 78 deg C to -10 deg C, within 1.5 h
2: H2 / Lindlar cat. / diethyl ether; hexane / 0.25 h / Ambient temperature
View Scheme
参考文献
Pelter, Andrew; Al-Bayati, Redha I. H.; Ayoub, Miqdad T.; Lewis, Wynn; Pardasani, Pushpa; Hansel, Rudolf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 717 - 742
hydrogen; Lindlar catalyst in diethyl ether; hexane
0.25 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Pelter, Andrew; Al-Bayati, Redha I. H.; Ayoub, Miqdad T.; Lewis, Wynn; Pardasani, Pushpa; Hansel, Rudolf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 717 - 742
