2,4-二溴-1,7-萘啶合成路线 (共 1 条)
反应条件
1.1: potassium tert-butylate / 18 h / 75 °C / Inert atmosphere
2.1: phosphorus oxytribromide; [C4C1Pyrr][CF3SO3] / 18 h / 85 °C
2.2: Cooling with ice
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参考文献
MERCK PATENT GMBH; DORSCH, Dieter; JONCZYK, Alfred; HOELZEMANN, Guenter; AMENDT, Christiane; ZENKE, Frank
Patent: WO2012/595 A1, 2012 ;
WO 2012/000595 A1