1,1’-[(4-硝基苯基)亚甲基]双[2,4,6-三甲氧基]-苯合成路线 （共 6 条）
反应条件
FeCl3·6H2O in dichloromethane
T=0 - 20°C; Friedel Crafts arylation; 3.5 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
tin(IV) chloride; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium
T=90°C; 1 h;
参考文献
Podder, Susmita; Choudhury, Joyanta; Roy, Ujjal Kanti; Roy, Sujit
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 3100 - 3103
反应条件
iodine in tetrahydrofuran
T=20°C; aza-Friedel-Crafts reaction;
参考文献
Jaratjaroonphong, Jaray; Krajangsri, Suppachai; Reutrakul, Vichai
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2476 - 2479
反应条件
iodine in toluene
T=20°C; aza-Friedel-Crafts reaction;
参考文献
Jaratjaroonphong, Jaray; Krajangsri, Suppachai; Reutrakul, Vichai
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2476 - 2479
反应条件
1: amberlite H+ resin IR-120 / toluene / 12 h / 120 °C / |Dean-Stark; |Molecular sieve
2: [Ir(COD)(SnCl3)Cl(μ-Cl)]2 / 1,2-dichloro-ethane / 0.75 h / 20 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Chatterjee, Paresh Nath; Maity, Arnab Kumar; Mohapatra, Swapna Sarita; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 13 p. 2816 - 2826
反应条件
1: amberlite H+ resin IR-120 / toluene / 12 h / 120 °C / |Dean-Stark; |Molecular sieve
2: [Ir(COD)(SnCl3)Cl(μ-Cl)]2 / 1,2-dichloro-ethane / 0.75 h / 20 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Chatterjee, Paresh Nath; Maity, Arnab Kumar; Mohapatra, Swapna Sarita; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 13 p. 2816 - 2826
