[(4-氯苯基)-异喹啉-1-甲基] 苯甲酸合成路线 （共 4 条）
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in acetonitrile
0.0833333 h; ultrasound sonication;
参考文献
Ezquerra, Jesus; Alvarez-Builla, Julio
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 917 - 925
反应条件
1,4-dioxane; diethyl ether
T=-10°C; und anschliessend mit aether.4-Chlor-benzaldehyd-Loesung;
参考文献
Walters et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1177,1181
反应条件
1: 69 percent / triethylbenzylammonmium chloride / CH2Cl2; H2O / 0.33 h / Irradiation; ultrasound sonication
2: 98 percent / 50percent aq. NaOH / triethylbenzylammonium chloride / acetonitrile / 0.08 h / ultrasound sonication
View Scheme
参考文献
Ezquerra, Jesus; Alvarez-Builla, Julio
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 917 - 925
反应条件
1: 69 percent / triethylbenzylammonmium chloride / CH2Cl2; H2O / 0.33 h / Irradiation; ultrasound sonication
2: 98 percent / 50percent aq. NaOH / triethylbenzylammonium chloride / acetonitrile / 0.08 h / ultrasound sonication
View Scheme
参考文献
Ezquerra, Jesus; Alvarez-Builla, Julio
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 917 - 925
