9,9-二对甲苯-9h-芴合成路线 （共 8 条）
反应条件
2: H2SO4 / aq. acetic acid / 15 - 35 °C
View Scheme
参考文献
Hart,H.; Sedor,E.A.
Journal of the American Chemical Society, 1967 , vol. 89, # 10 p. 2342 - 2347
反应条件
2: H2SO4 / aq. acetic acid / 15 - 35 °C
View Scheme
参考文献
Hart,H.; Sedor,E.A.
Journal of the American Chemical Society, 1967 , vol. 89, # 10 p. 2342 - 2347
反应条件
potassium tert-butylate; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene
T=100°C; 12 h; Schlenk techniqueInert atmosphereGlovebox; Catalytic behavior;
参考文献
Cao, Xiao; Yang, Weidong; Liu, Chao; Wei, Fuliang; Wu, Kun; Sun, Wei; Song, Juan; Xie, Linghai; Huang, Wei
Organic Letters, 2013 , vol. 15, # 12 p. 3102 - 3105
反应条件
lithium aluminium tetrahydride; NbCl5 in 1,4-dioxane
4 h; Heating;
参考文献
Fuchibe, Kohei; Akiyama, Takahiko
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1434 - 1435
反应条件
hydrogenchloride
Heating;
参考文献
Hart,H.; Sedor,E.A.
Journal of the American Chemical Society, 1967 , vol. 89, # 10 p. 2342 - 2347
参考文献
Vinogradova,S.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 183 - 184
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, # 1 p. 191 - 192
反应条件
potassium dichromate; sulfuric acid
T=270 - 280°C;
参考文献
Vinogradova,S.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 183 - 184
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, # 1 p. 191 - 192
反应条件
1: K2Cr2O7, H2SO4 / 270 - 280 °C
2: SOCl2
View Scheme
参考文献
Vinogradova,S.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 183 - 184
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, # 1 p. 191 - 192
