5,5-二甲基-[1,3]氧杂-2-酮合成路线 （共 8 条）
反应条件
pyridine; W(CO)6; iodine in dichloromethane
T=40°C; P=60800 Torr; 18 h;
参考文献
Diaz, Delmy J.; Hylton, Keisha-Gay; McElwee-White, Lisa
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 734 - 738
反应条件
sodium hydride in tetrahydrofuran
T=25°C; 2 h; Inert atmosphere;
参考文献
Paz, Jairo; Perez-Balado, Carlos; Iglesias, Beatriz; Munoz, Luis
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3037 - 3046
反应条件
triethylamine; acetyl chloride in dichloromethane
T=-40 - 20°C;
参考文献
Paz, Jairo; Perez-Balado, Carlos; Iglesias, Beatriz; Munoz, Luis
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3037 - 3046
反应条件
1: aq. NaN3
2: H2 / Pt-C / ethanol
3: NaOMe / 24 h / 150 - 170 °C
View Scheme
参考文献
Alewood,P.F. et al.
Canadian Journal of Chemistry, 1974 , vol. 52, p. 4083 - 4089
反应条件
1: H2 / Pt-C / ethanol
2: NaOMe / 24 h / 150 - 170 °C
View Scheme
参考文献
Alewood,P.F. et al.
Canadian Journal of Chemistry, 1974 , vol. 52, p. 4083 - 4089
反应条件
in tetrahydrofuran
18 h;
参考文献
Diaz, Delmy J.; Hylton, Keisha-Gay; McElwee-White, Lisa
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 734 - 738
参考文献
Diaz, Delmy J.; Hylton, Keisha-Gay; McElwee-White, Lisa
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 734 - 738
反应条件
sodium methylate
T=150 - 170°C; 24 h;
参考文献
Alewood,P.F. et al.
Canadian Journal of Chemistry, 1974 , vol. 52, p. 4083 - 4089
