2-甲基-2H-1,2-苯并异硒唑-3-酮合成路线 （共 9 条）
反应条件
in water
2 h; Ambient temperature;
参考文献
Pietka-Ottlik, Magdalena; Wojtowicz-Mlochowska, Halina; Kolodziejczyk, Katarzyna; Piasecki, Egbert; Mlochowski, Jacek
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 10 p. 1423 - 1427
反应条件
selenium; copper(l) iodide; 1,10-phenanthroline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 16 h; Inert atmosphere;
参考文献
Balkrishna, Shah Jaimin; Bhakuni, Bhagat Singh; Chopra, Deepak; Kumar, Sangit
Organic Letters, 2010 , vol. 12, # 23 p. 5394 - 5397
反应条件
dihydrogen peroxide in chloroform-d1
参考文献
Bhabak, Krishna P.; Mugesh, Govindasamy
Chemistry - An Asian Journal, 2009 , vol. 4, # 6 p. 974 - 983
反应条件
1: thionyl chloride / N,N-dimethyl-formamide / Reflux
2: dichloromethane
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 0 - 5 °C
1.2: -5 - 0 °C
2.1: thionyl chloride / N,N-dimethyl-formamide / Reflux
3.1: dichloromethane
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
mercury(II) diacetate
参考文献
Weber,R.; Renson,M.
Bulletin de la Societe Chimique de France, 1976 , p. 1124 - 1126
参考文献
Weber,R.; Renson,M.
Bulletin de la Societe Chimique de France, 1976 , p. 1124 - 1126
参考文献
Lesser; Weiss
Chemische Berichte, 1924 , vol. 57, p. 1079
反应条件
phosphorus pentachloride
参考文献
Weber,R.; Renson,M.
Bulletin de la Societe Chimique de France, 1976 , p. 1124 - 1126
