2-(4-甲氧苯基)乙胺合成路线 （共 112 条）
反应条件
1: 58 percent / Ni(acac)2/P(c-C6H11)(C6H5)2 / tetrahydrofuran / 1 h / 20 °C 2: 50 percent / LiAlH4, AlCl3 / diethyl ether / 1 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 1 p. 40 - 42
反应条件
titanium tetrachloride in tetrahydrofuran 2.5 h; Heating;
参考文献
Vellemaee, Eerold; Lebedev, Oleg; Maeeorg, Uno
Tetrahedron Letters, 2008 , vol. 49, # 8 p. 1373 - 1375
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 0.5 h; 2: With Amberlyst 15 in dichloromethane 1 h;
参考文献
Wild, Gareth. P.; Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.
Tetrahedron, 2009 , vol. 65, # 8 p. 1618 - 1629
反应条件
1: 86 percent / P-ph-phen*Pd(0), NaOAc / dimethylformamide; H2O / 12 h / 130 °C 2: H2 / 5percent Pd/C / ethanol / 12 h / 100 °C / 3040 Torr 3: 53 percent / NaOH, Br2 / H2O / 0.25 h / 70 - 80 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3563 - 3574
反应条件
1: H2 / 5percent Pd/C / ethanol / 12 h / 100 °C / 3040 Torr 2: 53 percent / NaOH, Br2 / H2O / 0.25 h / 70 - 80 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3563 - 3574
反应条件
hydrogenchloride; ethanol; platinum Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2593,2594
反应条件
hydrazine hydrate in methanol T=70°C;
参考文献
Journal of Physical Chemistry, , vol. 98, # 2 p. 412 - 419
反应条件
1: sodium azide / dimethylformamide / 20 °C 2: Ph3P; H2O / tetrahydrofuran / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 14 p. 4098 - 4115
反应条件
1: 72 percent 2: 70 percent / H2 / carbon palladium 10percent / 85 °C / 37503 Torr View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 18, # 4 p. 319 - 329
反应条件
chloroform; nitrosyl chloride Hydrieren des Reaktionsprodukts an Raney-Nickel in Methanol;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 234, p. 2617
Ann.scient.Univ.Besancon <2> Chimie, Nr.2.<1956>13,19
