N-甲基邻苯二甲酰亚胺合成路线 (共 249 条)
反应条件
acetamide T=140 - 160°C;
参考文献
Monatshefte fuer Chemie, , vol. 87, p. 526,531
参考文献
Helvetica Chimica Acta, , vol. 29, p. 1675,1677, 1681
反应条件
T=13°C; 25 h; Irradiation; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 50, # 3 p. 701 - 714
反应条件
in acetonitrile Elimination; 30 h; Irradiation;
参考文献
Tetrahedron, , vol. 55, # 41 p. 11997 - 12008
反应条件
1: 87 percent / K2CO3 / dimethylsulfoxide / 24 h / 30 - 60 °C 2: acetone / 1 h / 10 - 20 °C / Irradiation View Scheme
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1099 - 1118
反应条件
1.1: ozone / dichloromethane / -70 °C / Inert atmosphere 1.2: -70 - 20 °C 2.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 20 °C 3.1: methylamine / water; tetrahydrofuran / 5 - 23 °C View Scheme
反应条件
1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 20 °C 2: methylamine / water; tetrahydrofuran / 5 - 23 °C View Scheme
反应条件
1.1: ozone / dichloromethane / -70 °C / Inert atmosphere 1.2: -70 - 20 °C 2.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 20 °C 3.1: methylamine / water; tetrahydrofuran / 5 - 23 °C View Scheme
反应条件
1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 20 °C 2: methylamine / water; tetrahydrofuran / 5 - 23 °C View Scheme
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076