N-甲基邻苯二甲酰亚胺合成路线 (共 249 条)
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
1: thionyl chloride / dichloromethane / 6 h / 50 °C / |Inert atmosphere 2: water / 0 °C / |Inert atmosphere 3: dichloromethane / 1.5 h / 20 °C / |Inert atmosphere 4: acetone / 0.5 h / 20 °C 5: acetone / 3 h / 20 °C / 1050.11 Torr View Scheme
参考文献
Organometallics, , vol. 32, # 16 p. 4664 - 4676
参考文献
Journal of the American Chemical Society, , vol. 32, p. 115
参考文献
DE628829 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 366
反应条件
ethanol; water T=25°C; 14-taegige Einw. und folgendes Eindampfes;
参考文献
Chemische Berichte, , vol. 29, p. 2530
参考文献
Journal of Organic Chemistry, , vol. 22, p. 148
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 238, p. 2169
反应条件
sodium carbonate in water 0.25 h;
参考文献
Canadian Journal of Chemistry, , vol. 67, # 6 p. 998 - 1009