N-甲基邻苯二甲酰亚胺合成路线 （共 249 条）
反应条件
in acetonitrile
T=28°C; 11 h; Irradiationquenching experiment with fluorene, variation of DMB concentration, quenching study with biacetyl, product formation isotope effects, isotope effect on the rate of proton abstraction using DMB-d6; Quantum yieldMechanism;
参考文献
Mazzocchi, Paul H.; Klingler, Lori
Journal of the American Chemical Society, 1984 , vol. 106, p. 7567 - 7572
反应条件
in acetonitrile
Irradiation;
参考文献
Mazzocchi, P. H.; Klingler, L.; Edwards, M.; Wilson, P.; Shook, D.
Tetrahedron Letters, 1983 , vol. 24, # 2 p. 143 - 146
反应条件
1: Zn; AcOH / Heating
2: 58 percent / t-BuLi / tetrahydrofuran; pentane / -78 - 20 °C
View Scheme
参考文献
Guo; Schultz
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 2154 - 2157
反应条件
1: 80 percent / NaBH4, 3 M HCl / ethanol / 2 h / 0 - 5 °C
2: 74 percent / DPPA, Et3N / benzene
3: 65 percent / xylene / Heating
View Scheme
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154
反应条件
1: 72 percent
2: 1.) SOCl2 2.) tetrabutylammonium azide / 1.) SOCl2, benzene, 48 h, RT 2.) tetrabutylammonium azide, acetonitrile, 1 h, RT
3: 33 percent / xylene / Heating
View Scheme
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154
反应条件
3 h; also in the presence of phenanthrene; Mechanism;
参考文献
Maruyama, Kazuhiro; Kubo, Yasuo
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1426 - 1435
反应条件
1: Zn; AcOH / Heating
2: 69 percent / t-BuLi / tetrahydrofuran; pentane / -78 - 20 °C
View Scheme
参考文献
Guo; Schultz
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 2154 - 2157
反应条件
[2,2']bipyridinyl; bis(acetylacetonate)nickel(II) in 1,4-dioxane
T=95°C; 16 h; Inert atmosphere;
参考文献
Havlik, Sarah E.; Simmons, Jessica M.; Winton, Valerie J.; Johnson, Jeffrey B.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3588 - 3593
反应条件
sodium tetrahydroborate in water; isopropyl alcohol; toluene
T=0°C; 4 h; Yield given;
参考文献
Fichert, Thomas; Massing, Ulrich
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 5017 - 5018
反应条件
N,N-dimethylglycine potassium salt in water
T=15 - 20°C; 1 h; UV-irradiationInert atmosphere;
参考文献
Gallagher, Sonia; Hatoum, Fadi; Zientek, Nicolai; Oelgemoeller, Michael
Tetrahedron Letters, 2010 , vol. 51, # 28 p. 3639 - 3641
