4',6-二甲氧基-7-羟基异黄酮合成路线 (共 4 条)
反应条件
boron trifluoride diethyl etherate; acetic anhydride in diethyl ether; acetic acid
Heating;
参考文献
Jah, Hem Chandra; Zilliken, Fritz; Breitmaier, Eberhard
Angewandte Chemie, 1981 , vol. 93, # 1 p. 129 - 130
反应条件
1: T=50°C; 0.166667 h;
2: With methanesulfonyl chloride in N,N-dimethyl-formamide
T=80°C; 0.5 h;
参考文献
Goto, Hideyuki; Terao, Yoshiyasu; Akai, Shuji
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 4 p. 346 - 360
反应条件
O-methyl transferase from cell-free extract of Citrus mitis; [methyl-14C]-S-adenosyl-L-methionine; 2-hydroxyethanethiol in water; dimethyl sulfoxide
T=35°C; 0.5 h; pH 7.5 buffer; Product distribution;
参考文献
Brunet, Gunter; Ibrahim, Ragai K.
Phytochemistry (Elsevier), 1980 , vol. 19, p. 741 - 746
反应条件
O-methyl transferase from cell-free extract of Citrus mitis; [methyl-14C]-S-adenosyl-L-methionine; 2-hydroxyethanethiol in water; dimethyl sulfoxide
T=35°C; 0.5 h; pH 7.5 buffer; Product distribution;
参考文献
Brunet, Gunter; Ibrahim, Ragai K.
Phytochemistry (Elsevier), 1980 , vol. 19, p. 741 - 746