3-(2-甲氧基苯基)丙酸甲酯合成路线 （共 15 条）
参考文献
Lockett; Short
Journal of the Chemical Society, 1939 , p. 787,789
反应条件
1: sodium; ethanol 2: pyridine; SOCl2 3: ethanol; sodium iodide; copper (II)-sulfate 4: methanol. KOH-solution View Scheme
参考文献
Lockett; Short
Journal of the Chemical Society, 1939 , p. 787,789
反应条件
1: sodium; ethanol 2: pyridine; SOCl2 3: ethanol; sodium iodide; copper (II)-sulfate 4: methanol. KOH-solution 5: POCl3; tetrachloroethane / zuletzt bei Siedetemperatur View Scheme
参考文献
Lockett; Short
Journal of the Chemical Society, 1939 , p. 787,789
反应条件
sulfuric acid
2.5 h; RefluxInert atmosphere;
参考文献
Thuaud, Frederic; Kojima, Shuntaro; Hirai, Go; Oonuma, Kana; Tsuchiya, Ayako; Uchida, Takako; Tsuchimoto, Teruhisa; Sodeoka, Mikiko
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 9 p. 2771 - 2782
反应条件
Novozym 435; acylase I from Aspergillus melleus; amano lipase AK from pseudomonas fluorescens; lipase from wheat germ; papaine in toluene
T=40°C; 48 h; Enzymatic reaction; Mechanism;
参考文献
Zysk, Malgorzata; Zadlo, Anna; Brodzka, Anna; Wisniewska, Catalina; Ostaszewski, Ryszard
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 102, p. 225 - 229
反应条件
1: methanol; 3,4-dihydrobenzopyran-2-one With sodium methylate in methanol
T=20°C; 0.166667 h;
2: dimethyl sulfate With sodium methylate in methanol
T=20 - 40°C; 0.5 h;
参考文献
TOYAMA CHEMICAL CO., LTD.; Hirono, Shuichi; Shiozawa, Shunichi
Patent: EP1445249 A1, 2004 ;
Location in patent: Page 118-119 ;
反应条件
pyridine; tetrabutylammomium bromide; niobium bromide in N,N-dimethyl-formamide
Electrochemical reaction;
参考文献
De Mendonca Cavalcanti, Janesmar Camilo; Fonseca Goulart, Marilia Oliveira; Leonel, Eric; Nedelec, Jean-Yves
Tetrahedron Letters, 2002 , vol. 43, # 36 p. 6343 - 6345
反应条件
tetraethylammonium p-toluenesulfonate in acetonitrile
T=20°C; Electrolysis;
参考文献
Kise, Naoki; Iitaka, Shumei; Iwasaki, Keisuke; Ueda, Nasuo
Journal of Organic Chemistry, 2002 , vol. 67, # 24 p. 8305 - 8315
反应条件
1: H2 / 5 percent Pd/C / ethyl acetate
2: MeOH
View Scheme
参考文献
DeLong, Mitchell A.; Amburgey, Jack; Taylor, Cynthia; Wos, John A.; Soper, David L.; Wang, Yili; Hicks, Renee
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 14 p. 1519 - 1522
反应条件
ammonium cerium (IV) nitrate
T=20°C; 4 h; Inert atmosphere;
参考文献
Casey, Brian M.; Sadasivam, Dhandapani V.; Flowers II, Robert A.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1472 - 1479
