4-硫代尿苷2’,3’,5’-三乙酸酯合成路线 （共 7 条）
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone T=25°C;
参考文献
Crestini; Saladino; Bernini; Mincione
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7785 - 7788
反应条件
3,3-dimethyldioxirane in ethanol; dichloromethane; acetone T=25°C;
参考文献
Saladino, Raffaele; Crestini, Claudia; Occhionero, Francesca; Nicoletti, Rosario
Tetrahedron, 1995 , vol. 51, # 12 p. 3607 - 3616
反应条件
3,3-dimethyldioxirane in ethanol; dichloromethane; acetone T=25°C;
参考文献
Saladino, Raffaele; Crestini, Claudia; Occhionero, Francesca; Nicoletti, Rosario
Tetrahedron, 1995 , vol. 51, # 12 p. 3607 - 3616
反应条件
3,3-dimethyldioxirane in ethanol; dichloromethane; acetone T=25°C;
参考文献
Crestini; Saladino; Bernini; Mincione
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7785 - 7788
反应条件
1: 73 percent / dimethyldioxirane, NH3 / CH2Cl2; acetone / 25 °C 2: 93 percent / 2N methanol. NH3 / CH2Cl2 / 25 °C View Scheme
参考文献
Saladino, Raffaele; Crestini, Claudia; Bernini, Roberta; Frachey, Giuseppe; Mincione, Enrico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3053 - 3054
反应条件
ammonia in methanol 12 h;
参考文献
El-Tayeb, Ali; Qi, Aidong; Nicholas, Robert A.; Mueller, Christa E.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 8 p. 2878 - 2890
反应条件
1: 64 percent / dimethyldioxirane / CH2Cl2; acetone / 25 °C
2: 90 percent / 2N methanol. NH3 / CH2Cl2 / 25 °C
View Scheme
参考文献
Saladino, Raffaele; Crestini, Claudia; Bernini, Roberta; Frachey, Giuseppe; Mincione, Enrico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3053 - 3054
