4-(甲基硫代)-1-丁胺合成路线 （共 11 条）
反应条件
hydrazine in ethanol 3 h; Heating / reflux;
参考文献
Rajski, Scott R.; Mays, Jared Rae
Patent: US2013/116203 A1, 2013 ;
Location in patent: Paragraph 0090 ;
反应条件
lithium aluminium tetrahydride in diethyl ether 0.5 h; Reflux;
参考文献
Moon, Joon-Kwan; Kim, Jun-Ran; Ahn, Young-Joon; Shibamoto, Takayuki
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 11 p. 6672 - 6677
反应条件
lithium aluminium tetrahydride
参考文献
Benn, M. H.; Singh, Vinod K.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 940 - 942
参考文献
Justus Liebigs Annalen der Chemie, , vol. 392, p. 10
反应条件
1: 12.5 mmol / sodium hydroxide / CHCl3 2: 100 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.5 h View Scheme
参考文献
Moon, Joon-Kwan; Kim, Jun-Ran; Ahn, Young-Joon; Shibamoto, Takayuki
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 11 p. 6672 - 6677
反应条件
sodium hydroxide in dichloromethane T=0 - 20°C; 3.5 h;
参考文献
Rajski, Scott R.; Mays, Jared Rae
Patent: US2013/116203 A1, 2013 ;
Location in patent: Paragraph 0091 ;
反应条件
Yield given. Multistep reaction;
参考文献
Hu, Kun; Qi, Yan-Jie; Zhao, Juan; Jiang, He-Fei; Chen, Xin; Ren, Jie
European Journal of Medicinal Chemistry, 2013 , vol. 64, p. 529 - 539
反应条件
ethanol Oxydation des Reaktionsprodukts mit 0.5 Mol Jod in Aethanol, Einwirkung von Natriumaethylat-Loesung und erneute Oxydation mit 0.5 Mol Jod in Aethanol bei 0grad;
参考文献
Schmid; Karrer
Helvetica Chimica Acta, 1948 , vol. 31, p. 1497,1500
反应条件
2: aq. ethanol / 48 h / 27 °C / Helminthosporium species NRRL 4671 View Scheme
参考文献
Holland, Herbert L.; Brown, Frances M.; Larsen, Brett G.; Zabic, Mirjana
Tetrahedron: Asymmetry, 1995 , vol. 6, # 7 p. 1569 - 1574
反应条件
2: aq. ethanol / 48 h / 27 °C / Helminthosporium species NRRL 4671 View Scheme
参考文献
Holland, Herbert L.; Brown, Frances M.; Larsen, Brett G.; Zabic, Mirjana
Tetrahedron: Asymmetry, 1995 , vol. 6, # 7 p. 1569 - 1574
