1-(2,3-二氢-1H-吡咯里嗪-5-基)乙酮合成路线 （共 4 条）
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
T=95 - 100°C; Carbonylation; cyclization; P=60800 Torr;
参考文献
Miranda, Luis D.; Cruz-Almanza, Raymundo; Alvarez-Garcia, Abraham; Muchowski, Joseph M.
Tetrahedron Letters, 2000 , vol. 41, # 17 p. 3035 - 3038
反应条件
dihydrogen peroxide; iron(II) sulfate in dimethyl sulfoxide
T=40°C; Irradiation;
参考文献
Artis; Cho; Jaime-Figueroa; Muchowski
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2456 - 2466
反应条件
1: 93 percent / 87percent KOH / dimethylsulfoxide / 1.) sonication, 10 min, 2.) r.t.
2: 90 percent / NaI / acetonitrile / Heating
3: 50 percent / FeSO4*7H2O, 30percent aq. H2O2 / dimethylsulfoxide / 40 °C / Irradiation
View Scheme
参考文献
Artis; Cho; Jaime-Figueroa; Muchowski
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2456 - 2466
反应条件
1: 90 percent / NaI / acetonitrile / Heating
2: 50 percent / FeSO4*7H2O, 30percent aq. H2O2 / dimethylsulfoxide / 40 °C / Irradiation
View Scheme
参考文献
Artis; Cho; Jaime-Figueroa; Muchowski
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2456 - 2466
