反应条件
1: NaBH4 / ethanol / Ambient temperature
2: m-chloroperbenzoic acid / CH2Cl2 / 40 °C
3: 1) (CF3CO)2O / 1) CH2Cl2, 1 h, r.t. 2) 30 min, r.t., pH 4.0 (NaOAc or AcOH)
View Scheme
参考文献
Bonin, Martine; Romero, Jose Ricardo; Grierson, David S.; Husson, Henri-Philippe
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2392 - 2400