5-溴-2-羟基二苯甲酮合成路线 （共 11 条）
反应条件
AlCl3, aluminium chloride T=150°C; 3 h;
参考文献
MERCK SHARP and DOHME CORP.; MCCOMAS, Casey Cameron; LIVERTON, Nigel J.; HABERMANN, Joerg; KOCH, Uwe; NARJES, Frank; LI, Peng; PENG, Xuanjia; SOLL, Richard; WU, Hao; PALANI, Anandan; DAI, Xing; LIU, Hong; HE, Shuwen; DANG, Qung
Patent: WO2013/34048 A1, 2013 ;
Location in patent: Page/Page column 67; 68 ;
反应条件
thionyl chloride; AlCl3 in water; N,N-dimethyl-formamide; toluene; benzene
参考文献
Hamilton, Andrew D.; Ernst, Justin; Orner, Brendan P.
Patent: US2003/8882 A1, 2003 ;
反应条件
1: With dimethyl sulfoxide; trifluoroacetic acid; palladium diacetate T=95°C; 24 h; 2: With water T=70°C; 2 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3551 - 3558
反应条件
1: pyridine / diethyl ether 2: AlCl3, aluminium chloride / 2 h / 160 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 48, # 1 p. 230 - 236
反应条件
1: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / dichloromethane / 8 h / 20 °C / Inert atmosphere 2: AlCl3, aluminium chloride / N,N-dimethyl-formamide / 3 h / 210 °C View Scheme
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 6 p. 1939 - 1944
反应条件
sodium hydroxide T=80 - 85°C; 1 h;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 332, # 6 p. 1093 - 1098
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 21, # 5 p. 493 - 497
反应条件
sodium hydroxide T=80 - 85°C; 1 h; Product distribution;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 332, # 6 p. 1093 - 1098
反应条件
sodium hydroxide T=80 - 85°C; 1 h; Product distribution;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 332, # 6 p. 1093 - 1098
反应条件
1: NH2OH
2: methanol. sodium methylate
3: polyphosphoric acid
View Scheme
参考文献
Blatt
Journal of Organic Chemistry, 1955 , vol. 20, p. 591,599
