N-苄基-1-(4-溴苯基)甲胺合成路线 （共 13 条）
反应条件
TPP; oxygen in ethyl acetate T=20°C; P=760.051 Torr; 14 h; Molecular sieveIrradiation;
参考文献
Jiang, Gaoxl; Chen, Jian; Huang, Jie-Sheng; Che, Chi-Ming
Organic Letters, 2009 , vol. 11, # 20 p. 4568 - 4571
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=45°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Nicolaou; Mathison, Casey J. N.; Montagnon, Tamsyn
Angewandte Chemie - International Edition, 2003 , vol. 42, # 34 p. 4077 - 4082
反应条件
TPP; oxygen in ethyl acetate T=20°C; P=760.051 Torr; 14 h; Molecular sieveIrradiation;
参考文献
Jiang, Gaoxl; Chen, Jian; Huang, Jie-Sheng; Che, Chi-Ming
Organic Letters, 2009 , vol. 11, # 20 p. 4568 - 4571
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 23 h;
参考文献
Nicolaou; Mathison, Casey J. N.; Montagnon, Tamsyn
Journal of the American Chemical Society, 2004 , vol. 126, # 16 p. 5192 - 5201
反应条件
Co-phthalocyanine; (Ph)2SiH2 in ethanol
T=70°C; 12 h; chemoselective reaction;
参考文献
Kumar, Vishal; Sharma, Upendra; Verma, Praveen K.; Kumar, Neeraj; Singh, Bikram
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 870 - 878
反应条件
titanium(IV) isopropylate; CaH2; zinc dibromide in tetrahydrofuran
T=40°C; 12 h;
参考文献
Aida, Toshio; Kuboki, Norikatsu; Kato, Kenji; Uchikawa, Wataru; Matsuno, Chikashi; Okamoto, Sentaro
Tetrahedron Letters, 2005 , vol. 46, # 10 p. 1667 - 1669
反应条件
1,1,3,3-tetramethyldisiloxane; zinc trifluoromethanesulfonate in toluene
T=100°C; Inert atmosphere; chemoselective reaction;
参考文献
Das, Shoubhik; Addis, Daniele; Junge, Kathrin; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 43 p. 12186 - 12192
反应条件
1: With hydrogenchloride in diethyl ether
T=23°C; 1 h; Inert atmosphere;
2: With sodium hydrogencarbonate in methanol; water
T=23°C; 2 h; Inert atmosphere;
参考文献
Cheng, Chen; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11304 - 11307
反应条件
sodium tetrahydroborate in methanol
1 h; Heating;
参考文献
Rogez, Guillaume; Ribera, Belen Ferrer; Credi, Alberto; Ballardini, Roberto; Gandolfi, Maria Teresa; Balzani, Vincenzo; Liu, Yi; Northrop, Brian H.; Stoddart, J. Fraser
Journal of the American Chemical Society, 2007 , vol. 129, # 15 p. 4633 - 4642
反应条件
1: toluene / 0.5 h / Heating
2: NaBH4 / methanol / 1 h / Heating
View Scheme
参考文献
Rogez, Guillaume; Ribera, Belen Ferrer; Credi, Alberto; Ballardini, Roberto; Gandolfi, Maria Teresa; Balzani, Vincenzo; Liu, Yi; Northrop, Brian H.; Stoddart, J. Fraser
Journal of the American Chemical Society, 2007 , vol. 129, # 15 p. 4633 - 4642
