反应条件
1: 100 percent / triethylamine / CH2Cl2 / 3 h / 20 °C 2: Br2; acetic acid / 1.25 h / 20 °C 3: HCl / H2O; tetrahydrofuran / 1 h / Heating 4: 3.0 g / NaNO2; HCl / H2O / 6 h / Heating 5: 43 percent / POCl3 / 2 h / 100 °C 6: hydrazine monohydrate / ethanol / 72 h / 20 °C 7: 24 percent / CuSO4 / H2O / 2 h / Heating View Scheme
参考文献
Woods, Keith W.; Fischer, John P.; Claiborne, Akiyo; Li, Tongmei; Thomas, Sheela A.; Zhu, Gui-Dong; Diebold, Robert B.; Liu, Xuesong; Shi, Yan; Klinghofer, Vered; Han, Edward K.; Guan, Ran; Magnone, Shayna R.; Johnson, Eric F.; Bouska, Jennifer J.; Olson, Amanda M.; Jong, Ron de; Oltersdorf, Tilman; Luo, Yan; Rosenberg, Saul H.; Giranda, Vincent L.; Li, Qun
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 20 p. 6832 - 6846
