1-(3-乙酰基-2-羟基-5-甲基苯基)-乙酮合成路线 （共 4 条）
反应条件
1: With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C;
2: With AlCl3, aluminium chloride in dichloromethane
T=0 - 20°C; 120 h;
3: With hydrogenchloride; water
T=0 - 20°C; 1 h;
参考文献
KINACIA PTY LTD.
Patent: WO2004/16607 A1, 2004 ;
Location in patent: Page 32 ;
WO 2004/016607 A1
反应条件
aluminium trichloride in nitrobenzene
T=60°C; Diels-Alder reaction;
参考文献
Aromi, Guillem; Gamez, Patrick; Berzal, Paula Carrero; Driessen, Willem L.; Reedijk, Jan
Synthetic Communications, 2003 , vol. 33, # 1 p. 11 - 18
反应条件
aluminium trichloride in nitrobenzene
参考文献
Mandal, Sanat Kumar; Nag, Kamalaksha
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2429 - 2434
反应条件
carbon disulfide; aluminium trichloride
参考文献
Auwers
Justus Liebigs Annalen der Chemie, 1909 , vol. 364, p. 166
