反应条件
1: 91 percent / NaI / acetone
2: 1.) (i-C3H7)2NLi / 1.) THF, n-hexane, room temp., 3 h, 2.) 55 deg C, 12 h
3: 92 percent / Amberlyst H-15 / methanol / 1 h / 45 °C
4: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating
5: MnO2 / CH2Cl2 / 6 h / Ambient temperature
6: 1.) Mg/Hg / 1.) Et2O, 30 min, 2.) room temp., 1 h
View Scheme
参考文献
Cardillo, Giuliana; Orena, Mario; Porzi, Gianni; Sandri, Sergio
Gazzetta Chimica Italiana, 1980 , vol. 110, # 9/10 p. 523 - 526
