4-(叔丁基二甲基硅氧)环己酮合成路线 （共 17 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 6 h;
参考文献
Song, Zhen Lei; Wang, Bao Min; Tu, Yong Qiang; Fan, Chun An; Zhang, Shu Yu
Organic Letters, 2003 , vol. 5, # 13 p. 2319 - 2321
参考文献
Rath, Jean-Philippe; Eipert, Martin; Kinast, Stephan; Maier, Martin E.
Synlett, 2005 , # 2 art. no. G42904ST, p. 314 - 318
反应条件
1: With 1H-imidazole in N,N-dimethyl-formamide T=20°C; 2: With pyridinium chlorochromate in dichloromethane 1.5 h; Further stages.;
参考文献
Malapelle, Adeline; Coslovi, Anna; Doisneau, Gilles; Beau, Jean-Marie
European Journal of Organic Chemistry, 2007 , # 19 p. 3145 - 3157
反应条件
cerium(III) chloride; sodium iodide in acetonitrile deprotection; 1 h; Heating;
参考文献
Carreno, M. Carmen; Urbano, Antonio; Di Vitta, Claudio
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8320 - 8330
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water 3 h; Ambient temperature;
参考文献
McDonald, Chriss E.; Nice, Lois E.; Kennedy, Kenneth E.
Tetrahedron Letters, 1994 , vol. 35, # 1 p. 57 - 60
反应条件
1: 79 percent / KBrO4; CAN 2: 99 percent / imidazole View Scheme
参考文献
Synlett, , # 2 art. no. G42904ST, p. 314 - 318
反应条件
1: 62 percent / imidazole / dimethylformamide; tetrahydrofuran / 0 °C 2: 98 percent / pyridinium chlorochromate / CH2Cl2 / 6 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 5, # 13 p. 2319 - 2321
反应条件
1: imidazole / dimethylformamide / 20 °C 2: 81 percent / NaI; CeCl3*7H2O / acetonitrile / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8320 - 8330
反应条件
1: CeCl3*7H2O; NaBH4 / methanol / 0.5 h / 20 °C 2: imidazole / dimethylformamide / 20 °C 3: 81 percent / NaI; CeCl3*7H2O / acetonitrile / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8320 - 8330
反应条件
in 1,4-dioxane; water; dimethyl sulfoxide 12 h; Heating;
参考文献
Kametani, Tetsuji; Kondoh, Hirotsune; Honda, Toshio; Ishizone, Hiroyuki; Suzuki, Yukio; Mori, Wakako
Chemistry Letters, 1989 , p. 901 - 904
