3,4-二甲氧基-2-硝基苯甲醛合成路线 （共 21 条）
反应条件
1: nitronium tetrafluoroborate / dichloromethane / 24 h / -20 °C / Inert atmosphere
2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 25 h / 20 - 80 °C / Inert atmosphere
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参考文献
Turkman, Nashaat; Shavrin, Aleksander; Ivanov, Roman A.; Rabinovich, Brian; Volgin, Andrei; Gelovani, Juri G.; Alauddin, Mian M.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 18 p. 5698 - 5707
参考文献
Pschorr; Stoehrer
Chemische Berichte, 1902 , vol. 35, p. 4398
参考文献
MacDonald
Journal of the Chemical Society, 1948 , p. 376
参考文献
Hayduck
Chemische Berichte, 1903 , vol. 36, p. 2932,3528
反应条件
sulfuric acid; nitric acid
参考文献
de Lange
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 45
反应条件
1: acetone; permanganate
2: carbon disulfide; phosphorus pentachloride
3: carbon disulfide; ammonia
4: sodium hypobromite / 40 °C
5: iron; diluted acetic acid
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参考文献
Pisovschi
Chemische Berichte, 1910 , vol. 43, p. 2140
反应条件
sodium acetate in ethanol
8 h; Heating;
参考文献
Soni, Namita; Barthwal, J. P.; Gupta, T. K.; Bhalla, T. N.; Parmar, S. S.; Bhargava, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 785 - 788
反应条件
1: acetic acid anhydride / 100 °C
2: ferrosulfate; ammonia
3: pentyl nitrite / Diazotization.Behandeln mit Kupferpulver
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参考文献
Pschorr
Chemische Berichte, 1906 , vol. 39, p. 3115
反应条件
potassium permanganate
参考文献
Insole, Joan M.
Journal of Chemical Research, Miniprint, 1990 , # 12 p. 2831 - 2867
反应条件
1: alcoholic KOH-solution
2: concentrated hydrochloric acid
View Scheme
参考文献
Slotta; Lauersen
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 139, p. 220,228
