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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5517-61-3
合成路线
（共 5 条）
5517-61-3
→
反应条件
36791-04-5
利巴韦林
反应条件
1.1: 89 percent / DMAP; pyridine / 50 °C 2.1: 95 percent / AcOH; H2SO4 / 0.5 h / 20 °C 3.1: hexamethyldisilazane; ammonium sulfate / 16 h / Heating 3.2: 38 percent / stannic chloride / acetonitrile; CH2Cl2 / 18 h / 20 °C 4.1: 80 percent / NH3 / methanol / 24 h / 20 °C View Scheme
参考文献
Kim, Myong Jung; Jeong, Lak Shin; Kim, Joong Hyup; Shin, Ji Hye; Chung, Soon Yong; Lee, Sang Kook; Chun, Moon Woo
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 715 - 724
5517-61-3
→
反应条件
60084-10-8
噻唑呋林
反应条件
1: 89 percent / DMAP; pyridine / 50 °C 2: 95 percent / AcOH; H2SO4 / 0.5 h / 20 °C 3: 69 percent / stannic chloride / CH2Cl2 / 3 h / Heating 4: 71 percent / triethylamine / methanol / 2 h / 20 °C 5: 74 percent / bromotrichloromethane; 1,8-diazabicyclo[5.4.0]-undec-7-ene / CH2Cl2 / 16 h / 0 °C 6: 85 percent / NH3 / methanol / 24 h / 20 °C View Scheme
参考文献
Kim, Myong Jung; Jeong, Lak Shin; Kim, Joong Hyup; Shin, Ji Hye; Chung, Soon Yong; Lee, Sang Kook; Chun, Moon Woo
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 715 - 724
5517-61-3
→
反应条件
6974-32-9
1-乙酰基-2,3,5-三苯甲酰氧基-1-beta-D-呋喃核糖
反应条件
1: 89 percent / DMAP; pyridine / 50 °C 2: 95 percent / AcOH; H2SO4 / 0.5 h / 20 °C View Scheme
参考文献
Kim, Myong Jung; Jeong, Lak Shin; Kim, Joong Hyup; Shin, Ji Hye; Chung, Soon Yong; Lee, Sang Kook; Chun, Moon Woo
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 715 - 724
5517-61-3
→
反应条件
23316-67-8
1-氰基-2,3,5-三苯甲酰氧基-β-D-呋喃核糖
反应条件
1: 89 percent / DMAP; pyridine / 50 °C 2: 95 percent / AcOH; H2SO4 / 0.5 h / 20 °C 3: 69 percent / stannic chloride / CH2Cl2 / 3 h / Heating View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 23, # 4 p. 715 - 724
5517-61-3
→
反应条件
60084-09-5
2-(2,3,5-三-O-苯甲酰基-beta-D-呋喃核糖基)-4-噻唑羧酸乙酯
反应条件
1: 89 percent / DMAP; pyridine / 50 °C 2: 95 percent / AcOH; H2SO4 / 0.5 h / 20 °C 3: 69 percent / stannic chloride / CH2Cl2 / 3 h / Heating 4: 71 percent / triethylamine / methanol / 2 h / 20 °C 5: 74 percent / bromotrichloromethane; 1,8-diazabicyclo[5.4.0]-undec-7-ene / CH2Cl2 / 16 h / 0 °C View Scheme
参考文献
Kim, Myong Jung; Jeong, Lak Shin; Kim, Joong Hyup; Shin, Ji Hye; Chung, Soon Yong; Lee, Sang Kook; Chun, Moon Woo
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 715 - 724
