1: ortho-nitrobenzoic acid With cupric(II) carbonate in various solvent(s)
T=120°C; 0.5 h;
2: para-bromotoluene With potassium fluoride; palladium acetylacetonate; iso-propyldiphenylphoshine in various solvent(s)
T=120°C; 24 h; Further stages.;
参考文献
Goossen, Lukas J.; Rodriguez, Nuria; Melzer, Bettina; Linder, Christophe; Deng, Guojun; Levy, Laura M.
Journal of the American Chemical Society, 2007 , vol. 129, # 15 p. 4824 - 4833
in water
NaOH added successively to a soln. of Ag-salt and o-nitrobenzoic acid until pH 5; precipitate redissolved in hot water, slowly evapd. in the dark at roomtemp.;
