反应条件
1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / |Inert atmosphere; |Schlenk technique 2.1: palladium 10 on activated carbon; hydrogen / methanol / 2 h / 3102.97 Torr / |Schlenk technique; |Inert atmosphere 3.1: manganese(IV) oxide / dichloromethane / 1 h / 20 °C / |Inert atmosphere; |Schlenk technique 4.1: pyridine; 4-(N,N-dimethlyamino)pyridine / ethanol / 48 h / |Inert atmosphere; |Schlenk technique; |Reflux 4.2: 16 h / 20 °C / |Inert atmosphere; |Schlenk technique; |Reflux View Scheme
参考文献
Das, Sanjib; Harde, Rajendra L.; Shelke, Dnyaneshwar E.; Khairatkar-Joshi, Neelima; Bajpai, Malini; Sapalya, Ratika S.; Surve, Harshada V.; Gudi, Girish S.; Pattem, Rambabu; Behera, Dayanidhi B.; Jadhav, Satyawan B.; Thomas, Abraham
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 9 p. 2073 - 2078
