N-(2,6-二氯-3-甲基-苯基)-2-(3,4-二甲基苯基)硫基乙酰胺合成路线 （共 9 条）
反应条件
1: Et3N / CH2Cl2 / -78 deg to RT, RT, 2 h 2: LiAlH4 / diethyl ether / 48 h / Heating View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4907 - 4910
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0 - 20°C;
参考文献
Jandeleit, Bernd; Li, Yunxiao; Gallop, Mark A.; Zerangue, Noa; Virsik, Peter A.; Fischer, Wolf-Nicolas
Patent: US2009/82464 A1, 2009 ;
Location in patent: Page/Page column 45 ;
反应条件
1: in dichloromethane
T=20°C; 0.5 h; Inert atmosphere;
2: With water; sodium hydrogencarbonate in dichloromethane
Saturated solution; chemoselective reaction;
参考文献
Wakita, Natsumi; Hara, Shoji
Tetrahedron, 2010 , vol. 66, # 40 p. 7939 - 7945
反应条件
sodium tetrahydroborate in ethanol
T=25°C; 1 h;
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4907 - 4910
反应条件
3,3-dimethyldioxirane
参考文献
Akbalina; Zlotskii; Kabal'nova; Grigor'ev; Kotlyar; Shereshovets
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 7 p. 1120 - 1122
反应条件
1: 1.94 g / pyridine / 3 h / 60 °C
2: 1.38 g / NaIO4 / methanol; H2O / 65 h / 25 °C
3: 1.13 g / NaBH4 / ethanol / 1 h / 25 °C
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4907 - 4910
反应条件
1: 1.38 g / NaIO4 / methanol; H2O / 65 h / 25 °C
2: 1.13 g / NaBH4 / ethanol / 1 h / 25 °C
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4907 - 4910
反应条件
1-oxyl-2,2,5,5-tetramethyl-4-phenyl-Δ3-imidazoline 3-oxide; chlorine dioxide; potassium bromide in acetonitrile
T=35°C; 4 h; KineticsProduct distribution; Further Variations:TemperaturesReagents;
参考文献
Abdrakhmanova; Kabal'nova; Rol'nik; Yagafarova; Shereshovets
Russian Chemical Bulletin, 2004 , vol. 53, # 8 p. 1755 - 1760
反应条件
1: Et3N / CH2Cl2 / -78 deg to RT, RT, 2 h
2: LiAlH4 / diethyl ether / 48 h / Heating
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4907 - 4910
