1-(2-氟苯基)-3,3-双-甲基硫烷基丙酮合成路线 (共 1 条)
反应条件
1: carbon disulfide; 1-(2-fluoro-phenyl)-ethanone With sodium hydride in N,N-dimethyl-formamide; toluene
T=20°C; 0.5 h;
2: methyl iodide in N,N-dimethyl-formamide; toluene
2 h; Cooling with ice;
参考文献
Chen, Xue-Bing; Liu, Xi-Ming; Huang, Rong; Yan, Sheng-Jiao; Lin, Jun
European Journal of Organic Chemistry, 2013 , # 21 p. 4607 - 4613