5-溴-1H-吲唑-1-羧酸叔丁酯合成路线 （共 4 条）
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=20°C;
参考文献
ALCON MANUFACTURING, LTD.
Patent: US2008/153813 A1, 2008 ;
Location in patent: Page/Page column 24 ;
US 20080153813 A1
反应条件
hydrazine T=110°C; 16 h;
参考文献
D'Sidocky, Neil R.; Harris, Roy L.; Hegde, Sayee G.; Hilgraf, Robert; McCarrick, Margaret A.; McKie, Jeffrey A.; Mortensen, Deborah S.; Nadolny, Lisa; Perin-Ninkovic, Sophie M.; Sapienza, John J.; Wright, Jonathan L.
Patent: US2008/242694 A1, 2008 ;
Location in patent: Page/Page column 41 ;
US 20080242694 A1
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=95°C; 16 h;
参考文献
D'Sidocky, Neil R.; Harris, Roy L.; Hegde, Sayee G.; Hilgraf, Robert; McCarrick, Margaret A.; McKie, Jeffrey A.; Mortensen, Deborah S.; Nadolny, Lisa; Perin-Ninkovic, Sophie M.; Sapienza, John J.; Wright, Jonathan L.
Patent: US2008/242694 A1, 2008 ;
Location in patent: Page/Page column 41 ;
US 20080242694 A1
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
ALCON MANUFACTURING, LTD.
Patent: US2008/153813 A1, 2008 ;
Location in patent: Page/Page column 24 ;
US 20080153813 A1
