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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55276-59-0
合成路线
（共 9 条）
55276-59-0
→
反应条件
253-82-7
喹唑啉
+
99933-58-1
+
74-11-3
香橙素
反应条件
sodium hydroxide in dimethyl sulfoxide 1 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 4 p. 1351 - 1359
5190-68-1
4-氯喹唑啉
+
104-88-1
4-氯苯甲醛
→
反应条件
55276-59-0
反应条件
1,3-dimethyl-1H-benzo[d]imidazol-3-ium iodide; sodium hydride in tetrahydrofuran 1 h; Heating;
参考文献
Miyashita; Matsuda; Iijima; Higashino
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 1 p. 43 - 48
98512-26-6
→
反应条件
55276-59-0
反应条件
sodium hydroxide in methanol 0.5 h; Heating;
参考文献
Higashino, Takeo; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 4 p. 1351 - 1359
5190-68-1
4-氯喹唑啉
→
反应条件
55276-59-0
反应条件
sodium hydride in tetrahydrofuran 1 h; Heating;
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
104-88-1
4-氯苯甲醛
→
反应条件
55276-59-0
反应条件
1: 98 percent / n-BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / -78 °C 2: 85 percent / dimethylformamide / 3 h / Heating 3: 39 percent / NaH / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
1632-83-3
1-甲基苯并咪唑
→
反应条件
55276-59-0
反应条件
1: 83 percent / n-BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / -78 °C 2: 92 percent / dimethylformamide / 3 h / Heating 3: 77 percent / NaH / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
122155-24-2
→
反应条件
55276-59-0
反应条件
1: 85 percent / dimethylformamide / 3 h / Heating 2: 39 percent / NaH / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
92434-95-2
→
反应条件
55276-59-0
反应条件
1: 92 percent / dimethylformamide / 3 h / Heating 2: 77 percent / NaH / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
92736-32-8
→
反应条件
55276-59-0
反应条件
1: NaH / dimethylformamide 2: 88 percent / NaOH / methanol / 0.5 h / Heating View Scheme
参考文献
Higashino, Takeo; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 4 p. 1351 - 1359
