1: 81.1 percent / DIBAL / benzene; hexane / 12 h / Ambient temperature 2: 80 percent / PCC / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
DR. AUGUST WOLFF GMBH and CO. KG ARZNEIMITTEL; SOEBERDT, Michael; KNIE, Ulrich; ABELS, Christoph
Patent: WO2012/69605 A1, 2012 ;
Location in patent: Page/Page column 60 ;
1: diethoxyphosphoryl-acetic acid ethyl ester With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=0°C; 0.5 h;
2: 3-phenyl-propionaldehyde in dichloromethane
T=25°C; 16 h;
3: With hydrogenchloride in dichloromethane; water
参考文献
Institut Natinal de la Sante et de la Rechereche (Inserm)
Patent: US2006/205695 A1, 2006 ;
Location in patent: Page/Page column 15 ;
