3,4-二氢-2(1H)-喹啉酮合成路线 (共 181 条)
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in dimethyl sulfoxide T=120°C;
参考文献
Tetrahedron, , vol. 65, # 10 p. 1982 - 1987
反应条件
iron(III) chloride; acetic acid in dichloromethane Ambient temperature;
参考文献
Cherest, Marc; Lusinchi, Xavier
Tetrahedron Letters, 1989 , vol. 30, # 6 p. 715 - 718
反应条件
titanium(III) chloride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Kodera; Watanabe; Imada; Murahashi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 9 p. 2542 - 1549
反应条件
bis(acetylacetonate)nickel(II); triphenylphosphine in toluene T=60 - 80°C; 5 h;
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 646 - 666
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in dimethyl sulfoxide T=120°C;
参考文献
Zhou, Wang; Zhang, Liangren; Jiao, Ning
Tetrahedron, 2009 , vol. 65, # 10 p. 1982 - 1987
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium hydroxide in 1,4-dioxane; water 2 h; RefluxInert atmosphere;
参考文献
Horn, Joachim; Li, Ho Yin; Marsden, Stephen P.; Nelson, Adam; Shearer, Rachel J.; Campbell, Amanda J.; House, David; Weingarten, Gordon G.
Tetrahedron, 2009 , vol. 65, # 44 p. 9002 - 9007
反应条件
palladium 10 on activated carbon; zinc in water; tert-butyl alcohol T=150°C; 40 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in methanol; tert-butyl alcohol T=20 - 100°C; 16.25 h; Inert atmosphereSealed tube;
参考文献
Zhang, Lei; Sonaglia, Lorenzo; Stacey, Jason; Lautens, Mark
Organic Letters, 2013 , vol. 15, # 9 p. 2128 - 2131
反应条件
1-methyl-1H-imidazole; [2,2']bipyridinyl; 2,2,6,6-tetramethyl-piperidine-N-oxyl; copper(II) bis(trifluoromethanesulfonate); 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=60°C; 24 h; Molecular sieve;
参考文献
Green Chemistry, , vol. 14, # 5 p. 1281 - 1283
反应条件
aluminium trichloride; cyclohexane T=90°C; 24 h;
参考文献
Koltunov, Konstantin Yu.; Prakash, G. K. Surya; Rasul, Golam; Olah, George A.
Heterocycles, 2004 , vol. 62, p. 757 - 772