3,4-二氢-2(1H)-喹啉酮合成路线 (共 181 条)
反应条件
aluminium trichloride in dichloromethane T=-40 - 20°C; Beckmann rearrangement;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 10 p. 2205 - 2209
反应条件
tetrabutyl ammonium fluoride in dimethyl sulfoxide T=50°C;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 2163 - 2165
反应条件
tetrabutyl ammonium fluoride in dimethyl sulfoxide T=50°C;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 2163 - 2165
反应条件
tetrabutyl ammonium fluoride in dimethyl sulfoxide T=50°C;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 2163 - 2165
反应条件
1: pyridine 2: 17 percent / phenyliodine(III) bis(trifluoroacetate) / 3 h / 20 °C 3: 95 percent / hydrazine hydrate / ethanol / 1 h / Heating 4: 91 percent / Raney nickel W-2 / ethanol / 0.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 17 p. 6739 - 6744
反应条件
1: 17 percent / phenyliodine(III) bis(trifluoroacetate) / 3 h / 20 °C 2: 95 percent / hydrazine hydrate / ethanol / 1 h / Heating 3: 91 percent / Raney nickel W-2 / ethanol / 0.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 17 p. 6739 - 6744
反应条件
2: 96 percent / conc. H2SO4 3: 77 percent / H2 / PtO2 / acetic acid / Ambient temperature View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 329, # 6 p. 1063 - 1070
反应条件
hydrogenchloride; water in N,N-dimethyl-formamide
参考文献
Organic Letters, , vol. 11, # 5 p. 1043 - 1045
反应条件
methanol; sodium hydroxide in water T=80°C; 24 h;
参考文献
Synlett, , # 8 art. no. U00511ST, p. 1121 - 1124
反应条件
ethanol; nickel Hydrogenation.bis zur Aufnahme von 4 Mol Wasserstoff;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1442