3,4-二氢-2(1H)-喹啉酮合成路线 (共 181 条)
反应条件
1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate / tetrahydrofuran; water / 16 h / |Reflux 2: tri-ruthenium(0)dodecacarbonyl / chlorobenzene; N,N-dimethyl acetamide / 20 - 120 °C / |Sealed tube View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 3 p. 1125 - 1131
反应条件
potassium hydroxide; Pd(dpm)4Cl2 1.) H2O, 2.) H2O, 100 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 36, # 1 p. 125 - 128
反应条件
1: triflic acid / 5 h / 20 °C 2: 80 percent / AlCl3; cyclohexane / 24 h / 90 °C View Scheme
参考文献
Heterocycles, , vol. 62, p. 757 - 772
参考文献
Chemische Berichte, , vol. 15, p. 1422
反应条件
hydrogenchloride; ethanol
参考文献
in K.Ziegler,Praeparative Organische Chemie,Tl.I (= Naturf.Med.Dtschl.1935-1946,Bd.36)<Wiesbaden 1948> S.330
反应条件
sodium amalgam in alkal.Loesung und saeuert an;
参考文献
Chemische Berichte, , vol. 38, p. 3432
反应条件
1: sodium amalgam; alcohol 2: diluted mineral acid View Scheme
参考文献
Chemische Berichte, , vol. 15, p. 1422
反应条件
1: NaOH-solution 2: sodium amalgam / in alkal.Loesung und saeuert an View Scheme
参考文献
Chemische Berichte, , vol. 38, p. 3432
反应条件
1: alcohol; water; silver nitrate / weiteres Reagens: Natronlauge 2: sodium amalgam / in alkal.Loesung und saeuert an View Scheme
参考文献
Chemische Berichte, , vol. 38, p. 3432
反应条件
Ni(PPh3)4; triethylaluminum in toluene T=60 - 80°C; 5.5 h; without triethylaluminum; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1511 - 1518