N,N-双(2-氯乙基)苯胺合成路线 （共 26 条）
反应条件
sodium chloride in N,N-dimethyl-formamide T=160°C; 0.333333 h;
参考文献
Lin, Song-Wen; Sun, Qi; Ge, Ze-Mei; Wang, Xin; Ye, Jia; Li, Run-Tao
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 3 p. 940 - 943
反应条件
trichlorophosphate T=90°C; Inert atmosphereCooling with ice;
参考文献
Chen, Cheng; Wang, Ruyong; Guo, Liangqia; Fu, Nanyan; Dong, Haijun; Yuan, Yaofeng
Organic Letters, 2011 , vol. 13, # 5 p. 1162 - 1165
反应条件
thionyl chloride in toluene T=20 - 100°C; 1 h;
参考文献
EP1679069 A1, ;
Page/Page column 41 ;
反应条件
potassium iodide in acetonitrile T=110°C; P=825.066 Torr; 0.166667 h; microwave irradiation;
参考文献
Romera, Juan L.; Cid, Jose M.; Trabanco, Andres A.
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8797 - 8800
反应条件
1: calcium carbonate; water 2: phosphorus oxychloride View Scheme
参考文献
Journal of the Chemical Society, , p. 183,184
反应条件
sodium hydrogencarbonate; sodium iodide in ethylene glycol T=110°C; 1 h;
参考文献
Katz; Wilson, William L.; Scheller
Journal of the American Chemical Society, 1994 , vol. 116, # 15 p. 6636 - 6640
反应条件
tetra-n-butylammonium tribromide in dichloromethane T=10°C; 0.333333 h;
参考文献
Hoover, Lance R.; Pryor, Travis; Weitgenant, Jeremy A.; Williams, Peter E.; Storhoff, Bruce N.; Huffman, John C.
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 122, p. 155 - 166
参考文献
Ross; Warwick
Journal of the Chemical Society, 1956 , p. 1364,1366
反应条件
trichlorophosphate T=80°C; 2 h;
参考文献
Meng, Xiang-Ming; Liu, Lei; Hu, Hui-Yuan; Zhu, Man-Zhou; Wang, Mao-Xiang; Shi, Jin; Guo, Qing-Xiang
Tetrahedron Letters, 2006 , vol. 47, # 45 p. 7961 - 7964
反应条件
trichlorophosphate; benzene
参考文献
I.G. Farbenind.
Patent: DE711665 , 1935 ;
DRP/DRBP Org.Chem.
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Gen. Aniline Works
Patent: US2141090 , 1936 ;
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Anker; Cook
Journal of the Chemical Society, 1944 , p. 489,491
