1: oxalic acid dimethyl ester With sodium methylate in methanol
Claisen condensation; 0.25 h;
2: para-methylacetophenone in methanol
T=30°C; Claisen condensation; 0.0833333 h; Microwave irradiation;
参考文献
Reddy, Tummala R. K.; Li, Chan; Guo, Xiaoxia; Myrvang, Helene K.; Fischer, Peter M.; Dekker, Lodewijk V.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 7 p. 2080 - 2094
Bradshaw, Jerald S.; Jones, Brian A.; Nielsen, Ralph B.; Spencer, Neil O.; Thompson, Patricia K.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 957 - 962
methanol; diethyl ether; sodium
Behandeln mit verd. Schwefelsaeure;
参考文献
Wislicenus; Eble
Chemische Berichte, 1917 , vol. 50, p. 258
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Rising; Stieglitz
Journal of the American Chemical Society, 1918 , vol. 40, p. 728