反应条件
1.1: AlCl3 / CS2 / 16 h / 20 °C
2.1: 40.3 g / H2SO4 / H2O / 1 h / 80 °C
3.1: 66 percent / HNO3 / H2O / 0.08 h / -20 °C
4.1: 99 percent / NaBH4 / methanol / 0.17 h / 0 °C
5.1: 86 percent / TsOH / benzene / 16 h / Heating
6.1: O3 / CH2Cl2; methanol / -78 °C
6.2: Me2S; NaHCO3 / CH2Cl2; methanol / 4 h / 20 °C
6.3: 89 percent / NH3 / CH2Cl2; methanol; H2O / 16 h
7.1: 94 percent / NaOMe / dimethylformamide / 6 h / Heating
8.1: hydrazine monohydrate; Raney nickel / H2O; ethanol / 2 h / Heating
9.1: 34 percent / HOAc; NaNO2 / H2O / 0 - 20 °C
View Scheme
参考文献
Bryan Miller; Stowell, Joseph G; Dugar, Sundeep; Moock, Thomas E; Jenks, Christopher W; Farmer, Steven C; Phan, Bach; Wujcik, Chad E; Olmstead, Marilyn M
Tetrahedron, 2002 , vol. 58, # 30 p. 6061 - 6067
