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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55305-43-6
合成路线
（共 60 条）
55305-43-6
→
反应条件
68-34-8
对甲苯硫酰苯胺
+
64-10-8
苯基脲
+
104-15-4
对甲苯磺酸
反应条件
暂无反应条件数据
参考文献
Kurzer
Journal of the Chemical Society, 1949 , p. 1034,1036
1003-09-4
2-溴噻吩
+
55305-43-6
→
反应条件
1003-31-2
2-氰基噻吩
反应条件
1: thien-2-yl bromide With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
635-90-5
1-苯基吡咯
+
55305-43-6
→
反应条件
35524-46-0
1-苯基-1H-吡咯-2-甲腈
反应条件
boron trifluoride diethyl etherate in 1,2-dichloro-ethane T=80°C; 12 h; Sealed vialInert atmosphere; regioselective reaction;
参考文献
Yang, Yang; Zhang, Yan; Wang, Jianbo
Organic Letters, 2011 , vol. 13, # 20 p. 5608 - 5611
21702-84-1
2,4-二溴苯甲醚
+
55305-43-6
→
反应条件
144649-99-0
反应条件
1: 2,4-DBA With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=20°C; 4.16667 h; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
55305-43-6
+
460-00-4
→
反应条件
1194-02-1
反应条件
1: 1-bromo-4-fluorobenzene With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
2398-37-0
+
55305-43-6
→
反应条件
1527-89-5
反应条件
1: 3-methoxybromobenzene With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
19393-92-1
+
55305-43-6
→
反应条件
1194-65-6
反应条件
1: 1-bromo-2,6-dichlorobenzene With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=0°C; 1 h; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 15 p. 4217 - 4222
1072-85-1
+
106-38-7
+
55305-43-6
→
反应条件
114772-53-1
反应条件
1: para-bromotoluene With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: ortho-fluorobromobenzene With magnesium in tetrahydrofuran T=20 - 60°C; Inert atmosphere; 3: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
2635-13-4
+
55305-43-6
→
反应条件
4421-09-4
反应条件
1: 1,2-methylenedioxy-4-bromobenzene With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 15 p. 4217 - 4222
591-17-3
+
55305-43-6
→
反应条件
620-22-4
反应条件
1: 1-bromo-3-methyl-benzene With magnesium; lithium chloride in tetrahydrofuran T=20°C; Inert atmosphere; 2: N-cyano-N-phenyl-p-methylbenzenesulfonamide in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 15 p. 4217 - 4222
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