反应条件
1: 1.) LiHMDS / 1>) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, a) -78 deg C, 30 min, b) RT, 1.5 h
2: 1.) DIBAL-H, 2.) potassium sodium tartrate / 1.) CH2Cl2, toluene, -78 deg C, 1.5 h, 2.) CH2Cl2, toluene, MeOH, H2O, RT, 3 h
View Scheme
参考文献
Louwrier, Saskia; Tuynman, Antonin; Hiemstra, Henk
Tetrahedron, 1996 , vol. 52, # 7 p. 2629 - 2646
