您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-溴-1-壬醇
合成路线
（共 65 条）
55362-80-6
9-溴-1-壬醇
→
反应条件
173606-50-3
10-({[(2-甲基-2-丙基)氧基]羰基}氨基)癸酸
反应条件
1: 80 percent / Et3N, DMAP / CH2Cl2 2: 68 percent / dimethylsulfoxide 3: 80 percent / LiAlH4 4: 92 percent / Et3N / CH2Cl2 5: 76 percent / nBu4NF / tetrahydrofuran 6: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
55362-80-6
9-溴-1-壬醇
→
反应条件
34010-20-3
顺-9-十六烯醇乙酸酯
反应条件
1: 90 percent / acetonitrile 2: 71 percent / DMSO, NaY / tetrahydrofuran / 0.5 h 3: pyridine View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
55362-80-6
9-溴-1-壬醇
→
反应条件
1981-50-6
反应条件
1.1: acetonitrile / 48 h / |Inert atmosphere; |Reflux 2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 20 °C / |Inert atmosphere 2.2: 1 h / -78 °C / |Inert atmosphere 3.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / water; acetonitrile / 12 h / 20 °C View Scheme
参考文献
Bruns, Hilke; Thiel, Verena; Voget, Sonja; Patzelt, Diana; Daniel, Rolf; Wagner-Doebler, Irene; Schulz, Stefan
Chemistry and Biodiversity, 2013 , vol. 10, # 9 p. 1559 - 1573
55362-80-6
9-溴-1-壬醇
→
反应条件
20194-46-1
反应条件
1: 100 percent / p-toluenesulfonic acid / CHCl3 2: 45 percent / Heating 3: 1.) n-BuLi / 1.) THF, DMSO, hexane, RT, 30 min, 2.) THF, DMSO, hexane, RT, 3 h 4: 100 percent / H2 / PtO2 / methanol / Ambient temperature View Scheme
参考文献
Carballeira, Nestor; Thompson, Janice E.; Ayanoglu, Eser; Djerassi, Carl
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2751 - 2756
55362-80-6
9-溴-1-壬醇
→
反应条件
10378-01-5
(9Z)-9-十六碳烯-1-醇
反应条件
1: 90 percent / acetonitrile 2: DMSO, NaH / tetrahydrofuran / 0.5 h View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
55362-80-6
9-溴-1-壬醇
→
反应条件
173606-54-7
10-(t-叔丁氧羰基-氨基)-1-癸醇
反应条件
1: 80 percent / Et3N, DMAP / CH2Cl2 2: 68 percent / dimethylsulfoxide 3: 80 percent / LiAlH4 4: 92 percent / Et3N / CH2Cl2 5: 76 percent / nBu4NF / tetrahydrofuran View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
55362-80-6
9-溴-1-壬醇
→
反应条件
26543-36-2
10-十八碳炔酸甲酯
反应条件
1.1: toluene-4-sulfonic acid / dichloromethane / 20 °C 2.1: n-butyllithium / tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane / 0.5 h / -60 °C 2.2: -20 - 20 °C 3.1: Jone's reagent / acetone / 0 - 4 °C 4.1: sulfuric acid / 20 °C View Scheme
参考文献
Fu, Yu; Weng, Yue; Hong, Wen-Xu; Zhang, Qinghai
Synlett, 2011 , # 6 p. 809 - 812
55362-80-6
9-溴-1-壬醇
→
反应条件
23192-82-7
(E)-9-十四碳烯-1-醇乙酸酯
反应条件
1: 90 percent / acetonitrile 2: 63 percent / DMSO, NaH / tetrahydrofuran / 0.5 h 3: pyridine View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
55362-80-6
9-溴-1-壬醇
→
反应条件
651331-65-6
反应条件
1.1: NaH / tetrahydrofuran / Heating 2.1: acetonitrile / Heating 3.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C 3.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0.25 h / 0 °C 3.3: 74 percent / tetrahydrofuran; hexane / 2.5 h / -78 - 0 °C 4.1: 93 percent / H2 / Pd/C / ethanol / 4 h / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
55362-80-6
9-溴-1-壬醇
→
反应条件
651331-66-7
反应条件
1.1: NaH / tetrahydrofuran / Heating 2.1: acetonitrile / Heating 3.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 3.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 3.3: 65 percent / tetrahydrofuran; hexane / -78 - 0 °C 4.1: 91 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
首页
上一页
1
2
3
4
5
6
7
下一页
末页
到第
页
确定
