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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-溴-1-壬醇
合成路线
（共 65 条）
55362-80-6
9-溴-1-壬醇
→
反应条件
651331-67-8
反应条件
1.1: NaH / tetrahydrofuran / Heating 2.1: acetonitrile / Heating 3.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 3.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 3.3: 91 percent / tetrahydrofuran; hexane / -78 - 0 °C 4.1: 80 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
55362-80-6
9-溴-1-壬醇
→
反应条件
73674-10-9
反应条件
1: aq. HNO3 2: SOCl2 View Scheme
参考文献
Nakamura; Setodoi; Hanasaki
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 350, p. 93 - 101
55362-80-6
9-溴-1-壬醇
→
反应条件
77712-29-9
反应条件
2: 95 percent / dimethylsulfoxide / 15 h / 80 °C 3: 86 percent / NaOH, 3N HCl / ethanol / 19 h / Heating 4: PCl5 / CH2Cl2 / 2 h / 25 °C 5: 44 percent / AlCl3 / 1,2-dichloro-ethane / 72 h / 20 °C 6: 79 percent / NaOH / methanol / 2 h / Ambient temperature 7: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature 8: NaOH / methanol / 24 h / 5 °C View Scheme
参考文献
Goto; Okamoto; Okutani; Imada
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 10 p. 4422 - 4431
55362-80-6
9-溴-1-壬醇
→
反应条件
85920-71-4
反应条件
1: 88 percent / tetrahydrofuran / 4 h / Heating 2: 43 percent / LDA / tetrahydrofuran; hexane / 5 h / 0 deg C -> rt View Scheme
参考文献
Sims, Russell J.; Tischler, Samuel A.; Weiler, Larry
Tetrahedron Letters, 1983 , vol. 24, # 3 p. 253 - 256
55362-80-6
9-溴-1-壬醇
→
反应条件
875685-44-2
9-硝基油酸
反应条件
1: 67 percent / Jones' reagent / acetone; H2O / 0 °C 2: 92 percent / p-TsOH / toluene / Heating 3: 68 percent / AgNO2 / diethyl ether / 168 h / 20 °C 4: 81 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C 5: 86 percent / p-toluenesulfonic acid / 20 °C 6: 84 percent / Na2CO3 / benzene / 24 h / 80 - 90 °C 7: 95 percent / formic acid; Pd(PPh3)4 / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Woodcock, Steven R.; Marwitz, Adam J. V.; Bruno, Paulo; Branchaud, Bruce P.
Organic Letters, 2006 , vol. 8, # 18 p. 3931 - 3934
55362-80-6
9-溴-1-壬醇
→
反应条件
92038-37-4
反应条件
2: 95 percent / dimethylsulfoxide / 15 h / 80 °C 3: 86 percent / NaOH, 3N HCl / ethanol / 19 h / Heating View Scheme
参考文献
Goto; Okamoto; Okutani; Imada
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 10 p. 4422 - 4431
55362-80-6
9-溴-1-壬醇
→
反应条件
99828-63-4
反应条件
1.1: toluene-4-sulfonic acid / dichloromethane / 5 h / 0 - 20 °C 2.1: iodine; magnesium / tetrahydrofuran / 5.33 h / 20 °C / |Inert atmosphere; |Reflux 2.2: 12 h / 20 - 80 °C / |Ionic liquid 3.1: pyridinium p-toluenesulfonate / methanol / 50 °C 4.1: triphenylphosphine; carbon tetrabromide / dichloromethane / -10 °C View Scheme
参考文献
Zhang, Tao; Ma, Wei-Li; Li, Tian-Rui; Wu, Jia; Wang, Jun-Run; Du, Zhen-Ting
Molecules, 2013 , vol. 18, # 5 p. 5201 - 5208
55362-80-6
9-溴-1-壬醇
→
反应条件
463-24-1
9-氟-1-壬醇
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3 h;
参考文献
Tremblay, Amy E.; Buist, Peter H.; Hodgson, Derek; Dawson, Brian; Whittle, Ed; Shanklin, John
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 6 p. 629 - 632
55362-80-6
9-溴-1-壬醇
→
反应条件
52957-16-1
9,10-十四碳烯醇
反应条件
1: 90 percent / acetonitrile 2: DMSO, NaH / tetrahydrofuran / 0.5 h View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
110-87-2
3,4-二氢-2H-吡喃
+
55362-80-6
9-溴-1-壬醇
→
反应条件
55695-90-4
2-(9-溴壬基-1-氧基)四氢吡喃
反应条件
toluene-4-sulfonic acid in chloroform
参考文献
Carballeira, Nestor M.; Montano, Nashbly; Padilla, Luis F.
Chemistry and Physics of Lipids, 2007 , vol. 145, # 1 p. 37 - 44
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