(4-丁基苯基)(苯基)甲酮合成路线 （共 18 条）
反应条件
aluminium trichloride in carbon disulfide; water
参考文献
Kaken Chemical Co., Ltd.
Patent: US4124726 A1, 1978 ;
反应条件
copper(I) thiophene-2-carboxylate; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in diethyl ether T=20°C; 3 h;
参考文献
Ogawa, Daisuke; Hyodo, Keita; Suetsugu, Masato; Li, Jing; Inoue, Yoshiaki; Fujisawa, Mamoru; Iwasaki, Masayuki; Takagi, Kentaro; Nishihara, Yasushi
Tetrahedron, 2013 , vol. 69, # 12 p. 2565 - 2571
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in xylene T=130°C; Suzuki cross-coupling; 20 h;
参考文献
Kondolff, Isabelle; Doucet, Henri; Santelli, Maurice
Tetrahedron, 2004 , vol. 60, # 17 p. 3813 - 3818
反应条件
B-OMe-9-borabicyclo[3.3.1]nonane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran Heating;
参考文献
Fuerstner, Alois; Seidel, Guenter
Tetrahedron, 1995 , vol. 51, # 41 p. 11165 - 11176
反应条件
alkalimetal-zeolite in 2,2,4-trimethylpentane; benzene Irradiation2.) degassed at 1E-4 Torr and irradiated;
参考文献
Journal of the American Chemical Society, , vol. 110, # 14 p. 4848 - 4849
反应条件
alkalimetal-zeolite in 2,2,4-trimethylpentane; benzene Irradiation2.) degassed at 1E-4 Torr and irradiated;
参考文献
Journal of the American Chemical Society, , vol. 110, # 14 p. 4848 - 4849
反应条件
Cs-zeolite in 2,2,4-trimethylpentane; benzene Irradiation2.) degassed at 1E-4 Torr and irradiated;
参考文献
Journal of the American Chemical Society, , vol. 110, # 14 p. 4848 - 4849
反应条件
1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 2: dimethylsulfoxide-d6 / 0.5 h 3: aq. buffer / 0.25 h / |Inert atmosphere; |Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 3 p. 942 - 949
反应条件
1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 2: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 3: dimethylsulfoxide-d6 / 0.5 h 4: aq. buffer / 0.25 h / |Inert atmosphere; |Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 3 p. 942 - 949
反应条件
1.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C 1.2: 2 h / 3 - 20 °C 2.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 3.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 4.1: dimethylsulfoxide-d6 / 0.5 h 5.1: aq. buffer / 0.25 h / |Inert atmosphere; |Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 3 p. 942 - 949
