1-羟基-8-甲氧基-9,10-蒽醌合成路线 (共 30 条)
反应条件
T=130°C; sublimation in vac.;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; McKay, Peter G.
Tetrahedron Letters, 1981 , vol. 22, p. 701 - 702
反应条件
potassium hydroxide in pyridine; methanol
T=135°C; 4 h; Yield given;
参考文献
Takahashi; Terashima
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 12 p. 4539 - 4544
反应条件
chromium(VI) oxide; water; acetic acid
参考文献
Naylor; Gardner
Journal of the American Chemical Society, 1931 , vol. 53, p. 4114,4116
反应条件
1: concentrated sulfuric acid
2: acetic acid; CrO3; water
View Scheme
参考文献
Naylor; Gardner
Journal of the American Chemical Society, 1931 , vol. 53, p. 4114,4116
反应条件
1: 93 percent / K2CO3 / acetone / 5 h / Heating
2: 97 percent / 2 N NaOH / ethanol / 5 h
View Scheme
参考文献
Krohn; Muller; Priyono; et al.
1984 , vol. 1984, # 2 p. 306 - 318
反应条件
2,6-di-tert-butyl-phenol; N,N-diethylaniline
T=200°C; 4 h;
参考文献
Takahashi; Terashima
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 12 p. 4539 - 4544
反应条件
1-(tert-butyldimethylsilyloxy)-1-methoxyethene in acetonitrile
参考文献
Kraus, George A.; Walling, John A.
Tetrahedron Letters, 1986 , vol. 27, # 17 p. 1873 - 1876
反应条件
1: 2) Jones' reagent
2: H2C=C(OMe)SitBuMe2 / acetonitrile
View Scheme
参考文献
Kraus, George A.; Walling, John A.
Tetrahedron Letters, 1986 , vol. 27, # 17 p. 1873 - 1876
反应条件
1: 122 mg / CH2Cl2 / 672 h
2: 4 mg / 130 °C / 0.02 Torr
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; McKay, Peter G.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2095 - 2109
参考文献
Oesterle; Haugseth
Archiv der Pharmazie (Weinheim, Germany), 1915 , vol. 253, p. 337