1: With 1,2-dimethyl-1H-imidazole in dichloromethane
T=-45°C; 0.166667 h;
2: With tributyl-amine; titanium tetrachloride in dichloromethane
T=-45°C; 0.5 h;
参考文献
Misaki, Tomonori; Nagase, Ryohei; Matsumoto, Kunshi; Tanabe, Yoo
Journal of the American Chemical Society, 2005 , vol. 127, # 9 p. 2854 - 2855
lithium hexamethyldisilazane in tetrahydrofuran; toluene
T=60°C; Inert atmosphere;
参考文献
Rosenbaum, Anton I.; Cosner, Casey C.; Mariani, Christopher J.; Maxfield, Frederick R.; Wiest, Olaf; Helquist, Paul
Journal of Medicinal Chemistry, 2010 , vol. 53, # 14 p. 5281 - 5289
