in neat (no solvent, solid phase) byproducts: CO, CO2; thermal decomposition of Li2C2O4 in He, Ar, N2, CO and CO2 atmosphere, the heating rate was 6 deg/min; detd. by XRD and IR;
参考文献
Journal of Thermal Analysis, , vol. 32, p. 1229 - 1242
in neat (no solvent) LiOH*H2O and Ni acetate separately dissolved in H2O; mixed; pH adjusted to 8.5-9.5; heated at 110°C until they were dry; calcined at 300-500°C; monitored by X-ray diffraction;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 4 p. 515 - 519
in neat (no solvent) LiOH*H2O and Ni acetate separately dissolved in H2O; mixed; pH adjusted to 8.5-9.5; heated at 110°C until they were dry; calcined at 600°C; monitored by X-ray diffraction;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 4 p. 515 - 519
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反应条件
in water combustion synthesis; LiOH, H2SiO3, urea suspended in H2O, evapd., heated in air at 900-1100°C; not isolated, detected by XRD, IR;
参考文献
Journal of the American Ceramic Society, , vol. 88, # 7 p. 1720 - 1724
