反应条件
1.1: Grubb's 2nd generation catalyst / dichloromethane / 24 h / Inert atmosphere; Reflux 2.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 25 °C 3.1: pyridine / dichloromethane / 4 h / 25 °C / Inert atmosphere 4.1: toluene-4-sulfonic acid / methanol / 2 h / 25 °C / Inert atmosphere 4.2: 2 h / 25 °C / Inert atmosphere 5.1: sodium azide / N,N-dimethyl-formamide / 48 h / 90 °C / Inert atmosphere 6.1: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 67, # 48 p. 9283 - 9290
