in hydrogenchloride; water
addn. of stoichiometric amounts of aq. soln. of alkanaminium chloride to aq. HCl soln. of SnCl4*5H2O; filtration, washing with aq. HCl, drying in a vac. desiccator over NaOH and P2O5;
参考文献
Janiak, Tadeusz; Blazejowski, Jerzy
Thermochimica Acta, 1989 , vol. 141, p. 93 - 112
in hydrogenchloride
stoich. amts. of SnCl4 and Et3NHCl are mixed and dissolved in hydrochloric acid; recrystn. from hydrochloric acid by solvent evapn. in a desiccator, DTA;
in benzene
addn. of Et3NHCl to a soln. of the Ge compound in benzene; stirring at 20°C for 24 h;; detected by (1)H-NMR;;
参考文献
Riviere-Baudet, Monique; Morere, Alain; Onyszchuk, Mario; Satge, Jacques
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 70, # 1/2 p. 75 - 90
